Fractional Distillation Experiment

In the try out of distillment we sepa graded both miscible liquids. The object of distillation is to mark and purify compounds. We began our experiment by pose up an weapon for macroscale round-eyed distillation. We apply 60 ml of Cyclohexane/ toluene. We began with the temperature at 50 degrees Celsius. Unfortunately, we reached an error when the compounds evaporated similarly rapidly. The compounds evaporated so pronto that we lost information from 2 ml to 13 ml.The modify was lowered and as a go out we started to see a constant rate. From 14 ml to 18 ml it stayed at the rate of 90 degrees Celsius, from 19ml to 25 ml it was at 93 from 26ml to 38ml it stayed in the 90s for some(prenominal) minutes. When it reached the 50ml mark our temperature was at 108 degrees Celsius. Next we conducted the incomplete distillation experiment. We tightly packed the fractionating towboat with a cop metal sponge, poured our alloy into the 100 ml flask and waited for the change t o reach change state agitate.The boiling point temperature started at 83 degrees Celsius we then fall the temperature until we reached 25ml which was 82 degrees Celsius. Our results for the Toluene were 1. 4810 and 1. 4350 for the Cyclohexane. Unfortunately in the experiment for simple distillation, we reached an error when the compounds evaporated in any case rapidly. This was one kickoff of error that disarrayed our info. The compounds evaporated so chop-chop that we lost entropy from 2 ml to 13 ml. thus far though the data was not record it still was a successful experiment. This luxate has taught me to always funding a occlude eye on experiments no intimacy how slow the rate is. In the experiment of fractional distillation our results were reasonable scarcely I confide that if we would have laid the aluminum botch up around the fractionating column we could have decrease the temperature fluctuation during distillation.